Applications of low-temperature crystallography
dc.contributor.author | Billing, David Gordon | |
dc.date.accessioned | 2016-08-05T11:15:29Z | |
dc.date.available | 2016-08-05T11:15:29Z | |
dc.date.issued | 1991 | |
dc.description | A dissertation submitted to the Faculty of Science, University of the Witwatersrand, Johannesburg for the Degree of Master of Science January, 1991. | en_ZA |
dc.description.abstract | Two cryostats, a liquid nitrogen gas flow cryostat and a Be walled flow cryostat, suitable for use on Enraf Nonlus CAD4 four circle diffractometers have been commissioned and tested. The necessary techniques relating to crystal mounting and centring tor low-temperature data collection were also developed, The complete experimental procedure was tested by determining the crystal structures of the following three compounds at low-temperatures:N-arylpyrrolidin-2-one,4-p-hydroxyphenyl- 9,10,11-trihydroxy-8-ethyl-1,7-dioxaspiro[4,4]-nona-2,6-dione and 5,6-trans-Bromo- 5-hydroxy-3-nitrobicyclo[2,2.2]oct-2-ene.ln performing these structure determinations, some of the applications of low-temperature crystallography were considered. | en_ZA |
dc.format.extent | Online resource (110 leaves) | |
dc.identifier.citation | Billing, David Gordon (1991) Applications of low-temperature crystallography, University of Witwatersrand, Johannesburg, <http://wiredspace.wits.ac.za/handle/10539/20826> | |
dc.identifier.uri | http://hdl.handle.net/10539/20826 | |
dc.language.iso | en | en_ZA |
dc.subject.lcsh | Crystallography | |
dc.title | Applications of low-temperature crystallography | en_ZA |
dc.type | Thesis | en_ZA |
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